Chloroform Lab:
Chloroform Lab:
Introduction :
Chloroform is an important industrial product. There are two grade of chloroform. Anaesthatic amd technical grade chloroform or trichloromethane is at ordinary temp and pr. a heavy water , white volatile liq.
Having a pleasant, etheric, non irritant odor. It is not flammable but the hot vapour in a mixture with vapourised alcohol burns with a green organic solvent & lightly soluble in water, chloroform decompose at ordinary temp in sunlight in the absence of air and in the dark when air is present boiling point of chloroform is 61.3 digri C.
Manufacturing process :
There are three methods for making chloroform those are :-
1. By chlorination of methane.
2. From Acetone.
3. By reduction of carbon tetra chloride.
a . By chlorination of methane.
This process is the most important one . in fact the cholorinate process may so varrid as to product perponderane of any one of the chlormethanes one method used to obtain chloroform perdominantlly is to increase the chlorine methane ratio.
Required Machinery :
1. Acetone storage tank M.S 10,000 litter capacity. 1 no
2. S.S. distillation with condenser & other fitting. 1 set
3. Reactor SS capacity - 3000 lt 1 no.
4. Condensate storage tank 1 no.
5. Acidifier MS Constructive with lead lining. 1 no.
6. Distillation steel 1 no.
7. Chloroform storage tank. 1 no
8. Filter process. 2 nos.
9. Pumps valve, pipe line & others ancillaries ------
10. Office and Laboratory equipments -----
Introduction :
Chloroform is an important industrial product. There are two grade of chloroform. Anaesthatic amd technical grade chloroform or trichloromethane is at ordinary temp and pr. a heavy water , white volatile liq.
Having a pleasant, etheric, non irritant odor. It is not flammable but the hot vapour in a mixture with vapourised alcohol burns with a green organic solvent & lightly soluble in water, chloroform decompose at ordinary temp in sunlight in the absence of air and in the dark when air is present boiling point of chloroform is 61.3 digri C.
Manufacturing process :
There are three methods for making chloroform those are :-
1. By chlorination of methane.
2. From Acetone.
3. By reduction of carbon tetra chloride.
a . By chlorination of methane.
This process is the most important one . in fact the cholorinate process may so varrid as to product perponderane of any one of the chlormethanes one method used to obtain chloroform perdominantlly is to increase the chlorine methane ratio.
Required Machinery :
1. Acetone storage tank M.S 10,000 litter capacity. 1 no
2. S.S. distillation with condenser & other fitting. 1 set
3. Reactor SS capacity - 3000 lt 1 no.
4. Condensate storage tank 1 no.
5. Acidifier MS Constructive with lead lining. 1 no.
6. Distillation steel 1 no.
7. Chloroform storage tank. 1 no
8. Filter process. 2 nos.
9. Pumps valve, pipe line & others ancillaries ------
10. Office and Laboratory equipments -----
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